Separated local field spectroscopy of columnar and nematic liquid crystals.

نویسندگان

  • Sergey V Dvinskikh
  • Herbert Zimmermann
  • Arnold Maliniak
  • Dick Sandström
چکیده

We are in this work comparing the efficiencies of various 1H-13C separated local field (SLF) experiments when applied to columnar and nematic liquid crystals. In particular, the performances of the conventional SLF, proton-detected local field (PDLF), and polarization inversion spin exchange at the magic angle (PISEMA) methods in terms of spectral resolution, robustness, and ability to measure long-range couplings are investigated. The PDLF sequence provides in most cases the best dipolar resolution. This is especially obvious for weakly coupled 1H-13C spin pairs.

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عنوان ژورنال:
  • Journal of magnetic resonance

دوره 163 1  شماره 

صفحات  -

تاریخ انتشار 2003